UPR 5301

Rhéologie
bandeau cermav
Home / The research / Technical platforms

Physico-chemical characterization of polysaccharides in solution and hydrogels

This technical platform includes the following instruments: Stress-controlled rheometers, Strain-controlled rheometer, Capillary Viscometer, Viscometer based on the Couette principle, Tensile testing machine, Drop tensiometer, DSC microcalorimeter, Thermogravimetry...

Stress-controlled rheometers:

AR2000 and AR2000ex (TA instruments)
Investigation of the rheological behavior in oscillatory and steady shear flow of polysaccharide solutions and gels. Measurement of dynamic moduli (G’, G”) as a function of frequency and temperature. Creep. Normal force measurement (AR2000).

Strain-controlled rheometer:

ARES-RFS (TA Instruments)
Investigation of the rheological behavior in oscillatory and steady shear flow of polysaccharide solutions and gels. Measurement of dynamic moduli (G’, G”) as a function of frequency and temperature. Stress relaxation. Normal force measurement. 

De Gauche à droite : AR2000, AR2000ex, ARES-RFS
From left to right: AR2000, AR2000ex, ARES-RFS

Viscometer based on the Couette principle:

Low Shear 30 (Contraves)
Measurements of the viscosity for low viscous samples (viscosity from 1 mPa.s). Shear rates from 10-2 to 128 s-1. Measurements at fixed temperatures (15-80°C).

Capillary Viscometer

(SCHOTT Instruments): 
Determination of the intrinsic viscosity by automatic dilution of solutions. Measurements at fixed temperatures (15-80°C).

De gauche à droite : Viscosimètre à géométrie Couette, Viscosimètre capillaire.
From left to right: Viscometer based on the Couette principle, Capillary viscometer.

Tensile testing machine

(Shimadzu)
Investigation of the mechanical properties of polysaccharide films and hydrogels in both tension and compression.

Drop tensiometer

(IT concept)
Measurements of the surface tension and interfacial tension.

Elongational viscoelasticity (determination of the interface moduli E’ and E” according to the frequency). Contact angles. Fixed temperatures (15-80°C).

De gauche à droite : Machine de traction, Tensiomètre à goutte.
From left to right: Tensile testing apparatus, Drop tensiometer.

Thermogravimetry

(Setaram)
Analysis on 10 mg of sample. Temperature: 20 to 450°C.

DSC microcalorimeter

(Setaram)
Study of reactions involving biomacromolecules or conformational changes that lead to a change in energy (release (exothermic) or absorption (endothermic) of heat).

0.9 mL cells.

De gauche à droite : Appareil d’analyse thermogravimétrique, Microcalorimètre (DSC)
rom left to right, Thermogravimetric analysis system, Microcalorimeter (DSC).

Access conditions

The platform is open to public laboratories and private companies.

Physico-chemical characterization of polysaccharides in solution and hydrogels – Centre de recherches sur les macromolécules

Contact :

Rachel Auzély Velty, Professeur, responsable scientifique, 04 76 03 76 71